HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 4-(Butylsulfanyl)-2-nitroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1-Acetamido-4-n-butylthio-2-nitrobenzene | HCID 53804697 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-(Butylsulfanyl)-2-nitroaniline | HCID 11031561 | — |
Reaction Steps
3 G. of 1-acetamido-4-n-butylthio-2-nitrobenzene (prepared according to Example I) is hydrolyzed by treatment with 6 ml. 5N NaOH and 6 ml. ethanol on the steam bath for one hour. The mixture is concentrated and extracted with chloroform. Removal of the solvent leaves 1-amino-4-n-butylthio-2-nitrobenzene as a red oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072696 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-d46ab91787544e69aac2ccfb28b4f5e8 |
| Source note | uspto-grants-1978_02 |