HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 20371016, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 20371118 | HCID 20371118 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20371016 | HCID 20371016 | — |
Reaction Steps
0.7 G. of 2-amino-4-n-butylthio-1-(3-methoxycarbonyl-2-thioureido)benzene is dissolved in 20 ml. tetrahydrofuran and treated with 1.5 ml. of acetyl chloride. The mixture is stripped after two hours and the residue recrystallized from methanol, yielding pure 2-acetamido-4-n-butylthio-1-(3-methoxycarbonyl-2-thioureido)benzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072696 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-af11137e9cae46e491655a944e16f4f3 |
| Source note | uspto-grants-1978_02 |