Acetyl chloride → HCID 20371085, compound

Participants

Reaction Steps

0.7 G. of 2-amino-1-(3-methoxycarbonyl-2-thioureido)-5- phenylthiobenzene, as prepared according to Example XI, is dissolved in 20 ml. tetrahydrofuran and treated with 1.5 ml. of acetyl chloride. The mixture is stripped after two hours and the residue recrystallized from methanol, yielding 2-acetamido-1-(3-methoxycarbonyl-2-thioureido)-5-phenylthiobenzene.

Provenance & Evidence