HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methoxycarbonyl isothiocyanate → HCID 20371203, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methoxycarbonyl isothiocyanate | HCID 552246 | — |
| Reactant | HCID 20371006 | HCID 20371006 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20371203 | HCID 20371203 | — |
Reaction Steps
1 G. of 2-acetamido-1-amino4-phenylsulfinylbenzene in 30 ml. acetone is treated overnight with 2 g. methoxycarbonyl isothiocyanate. The solution is concentrated and the residue triturated with ether. Recrystallization yields 2-acetamido-1-(3-methoxycarbonyl-2-thioureido)-4-phenylsulfinylbenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072696 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-8046cf01ebc141c589772ea1be80349e |
| Source note | uspto-grants-1978_02 |