Methanol → HCID 20371170, compound

Participants

Reaction Steps

2 G. of 1-acetamido-2-nitro-4-propargylsulfinylbenzene is treated in a refluxing mixture of 160 ml. methanol and 40 ml. water with 4 g. iron powder (added in two portions) and 1 g. ferrous sulfate for four hours. The mixture is filtered, and the filtrated concentrated. The residue is dissolved in chloroform and washed with water, then the solvent evaporated affording 1-acetamido-2-amino-4-propargylsulfinylbenzene.

Provenance & Evidence