HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → 2-Acetamido-4-carbamoylthio-1-(3-methoxycarbonyl-2-thioureido)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 2-Amino-4-carbamoylthio-1-(3-methoxycarbonyl-2-thioureido)benzene | HCID 20371064 | — |
| Product | 2-Acetamido-4-carbamoylthio-1-(3-methoxycarbonyl-2-thioureido)benzene | HCID 20371226 | — |
Reaction Steps
0.7 G. of 2-amino-4-carbamoylthio-1-(3-methoxycarbonyl-2-thioureido)benzene is treated with 1.5 ml. of acetyl chloride. The mixture is stripped after two hours and the residue recrystallized to afford 2-acetamido-4-carbamoylthio-1-(3-methoxycarbonyl-2-thioureido)benzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072696 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-3f2cfe460997497d8fb91d84c732d43c |
| Source note | uspto-grants-1978_02 |