HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-Phenoxybenzene-1,2-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-Acetamido-2-amino-4-phenoxybenzene | HCID 20371094 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-Phenoxybenzene-1,2-diamine | HCID 10655643 | — |
Reaction Steps
1-Acetamido-2-amino-4-phenoxybenzene is treated with hydrochloric acid in aqueous methanol to afford 1,2-diamino-4-phenoxybenzene which, in turn, is reacted with methoxycarbonyl isothiocyanate in accordance with the technique set forth in the third paragraph of Example XIV to afford 1,2-bis(3-methoxycarbonyl-2-thioureido)-4-phenoxybenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072696 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-bd1c84df3a2d494b9fbf89ce0932367a |
| Source note | uspto-grants-1978_02 |