HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 616142Generated: October 29, 2026
Potassium Carbonate → 4-(2-Phenoxyethoxy)-2-nitroaniline
https://huagongshe.com/reaction/616142
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzene, (2-bromoethoxy)- | HCID 68526 | — |
| Reactant | N-(4-hydroxy-2-nitrophenyl)acetamide | HCID 4024832 | — |
| Product | 4-(2-Phenoxyethoxy)-2-nitroaniline | HCID 20545456 | — |
Reaction Steps
A mixture of 2.0 g. of 4-acetamido-3-nitrophenol, 2.2 g. of β-bromophenetole, 3 g. of potassium carbonate, and 20 ml. of dimethylformanide is heated under nitrogen for 16 hours at 110° C. The mixture is cooled and poured into ice water. The precipitated solid is collected, washed with water, and dried to give 2-nitro-4-(2-phenoxyethoxy)-aniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04072696 |
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| Source dataset | uspto-grants-1978_02 |
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| ORD ID | ord-d6c4abd5e9e343c89e5139cc4f534259 |
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| Source note | uspto-grants-1978_02 |
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