反应详情

温度

110 °C

A mixture of 2.0 g. of 4-acetamido-3-nitrophenol, 2.2 g. of β-bromophenetole, 3 g. of potassium carbonate, and 20 ml. of dimethylformanide is heated under nitrogen for 16 hours at 110° C. The mixture is cooled and poured into ice water. The precipitated solid is collected, washed with water, and dried to give 2-nitro-4-(2-phenoxyethoxy)-aniline.

1. additionA mixture of 2.0 g
2. temperatureThe mixture is cooled
3. customThe precipitated solid is collected
4. washwashed with water
5. customdried