HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 20371578, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 20371579 | HCID 20371579 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20371578 | HCID 20371578 | 165.9% |
Reaction Steps
3 g of α-(3,4-dimethoxyphenethylamino)-2-benzyloxyacetophenone hydrochloride, 0.7 g of sodium borohydride and 30 ml of ethanol are treated in the same manner as described in Example 1-(b). 2.5 g of α-(3,4-dimethoxyphenethylaminomethyl)-2-benzyloxybenzylalcohol hydrochloride are obtained. M.p. 115° - 117° C (recrystallized from a mixture of ethanol and ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072759 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-d82c9b31f94648f4a92de5cea51c3ea1 |
| Source note | uspto-grants-1978_02 |