HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 20371691, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 20371686 | HCID 20371686 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20371691 | HCID 20371691 | — |
Reaction Steps
In substantially the same manner as described above in Example 35 3-(4-methoxybenzamido)-4-hydroxy-α-(tert.butylaminomethyl)benzylalcohol hydrobromide was brominated with bromine in glacial acetic acid. The analytically pure title compound was precipitated from the reaction mixture with ether. M.p. 168° - 169.6° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072760 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-452e851098aa4cedb9890be978af2f4f |
| Source note | uspto-grants-1978_02 |