Hydrochloric Acid → HCID 86733248, compound

HRID 616277Notes

Reaction equation

HRID 616277 reaction equation
[CH2:1]([N:3]=[C:4](OC)[CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7])[CH3:2].[CH2:13]([NH2:15])[CH3:14].[ClH:16]>C(OCC)C>[ClH:16].[CH2:1]([NH:3][C:4](=[N:15][CH2:13][CH3:14])[CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7])[CH3:2]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 6341EthylamineHCID 20369368HCID 20369368, compound

Product 1

HCID 86733248HCID 86733248, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

To a solution of 3.46 g. (0.02 mole) of methyl N-ethyl-carbethoxyacetimidate in 30 ml. of diethyl ether is added 900 mg. (0.02 mole) of ethylamine and the reaction mixture allowed to stir several hours at room temperature. Anhydrous hydrogen chloride gas is slowly introduced into the reaction mixture until the formation of the amidine hydrochloride ceases. The product is filtered and dried in vacuo.

Workup

  1. filtrationThe product is filtered
  2. customdried in vacuo

Sources & evidence

ORD record
ord-15364276f2eb4002885ff51f6472f817
Source dataset
uspto-grants-1978_02
Patent number
US04073783

Reaction notes

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