HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-2-(diethylamine)ethane hydrochloride → Ethanamine, N,N-diethyl-2-(2-(2-methylpropoxy)phenoxy)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-2-(diethylamine)ethane hydrochloride | HCID 13363 | — |
| Reactant | 2-Isobutoxyphenol | HCID 691161 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethanamine, N,N-diethyl-2-(2-(2-methylpropoxy)phenoxy)- | HCID 3042674 | — |
Reaction Steps
The compound was prepared as described in Example 1, using sodium (2.3 g; 100 mole), o-isobutoxyphenol (8.30 g; 50 mmole) and diethylaminoethylchloride hydrochloride (8.6 g; 50 mmole) in 150 ml of ethanol. Yield 9.3 g (70%) of product, boiling at 112° C under a pressure of 0.01 mm Hg, nD25 : 1.4942.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04073917 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-b951a5f7c3754c21877343fa0b8cdfbc |
| Source note | uspto-grants-1978_02 |