HRID616449

反应详情

EQUATION

反应方程式

HRID 616449 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 1-bromocyclopentanecarboxylic acid (5.1 g) in ethanol (40 ml) containing concentrated sulphuric acid (10 drops) was refluxed for 4 hours. The solvent was removed by evaporation and the residual oil was partitioned between ether (50 ml) and 2N sodium carbonate (30 ml).

WORKUP

后处理

  1. temperaturewas refluxed for 4 hours
  2. customThe solvent was removed by evaporation
  3. customthe residual oil was partitioned between ether (50 ml) and 2N sodium carbonate (30 ml)