HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl 1-bromocyclopentane-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 1-Bromocyclopentane-1-carboxylic acid | HCID 13411841 | — |
| Catalyst | Sulfuric Acid | HCID 1118 | — |
| Product | Ethyl 1-bromocyclopentane-1-carboxylate | HCID 15301050 | — |
Reaction Steps
A solution of 1-bromocyclopentanecarboxylic acid (5.1 g) in ethanol (40 ml) containing concentrated sulphuric acid (10 drops) was refluxed for 4 hours. The solvent was removed by evaporation and the residual oil was partitioned between ether (50 ml) and 2N sodium carbonate (30 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04074047 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-705e73bf52aa4933af22a86f6e48dc6c |
| Source note | uspto-grants-1978_02 |