HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 20367579, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | HCID 85942030 | HCID 85942030 | — |
| Product | HCID 20367579 | HCID 20367579 | 88.1% |
Reaction Steps
Using the procedure of Example I, part F, 81.7 g of 3-amino-2-cyano-3-(1-pyrrolidinyl)propenethioamide were oxidized with 48 ml of 30% hydrogen peroxide to give 71.2 g of 5-amino-4-cyano-3-(1-pyrrolidinyl)isothiazole, m.p. 198°. The nmr spectrum was consistent with the assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04075001 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-a702880a3c2448678fd4e1cac4dfa48a |
| Source note | uspto-grants-1978_02 |