Nitrogen fluoride (N2F4) → 1,1,1,3,3,3-Hexafluoro-2-{[1,1,1,3,3,3-hexafluoro-2-(trifluoromethyl)propan-2-yl]peroxy}-2-(trifluoromethyl)propane

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Reaction Steps

In accordance with this invention, it has been found that the above-described objects can be accomplished by effecting a photolytic reaction between equimolar amounts of perfluoro-t-butyl hypofluorite and tetrafluorohydrazine. The resulting volatile reaction product, NF3, is evacuated at -90° C leaving a pure bis(perfluoro-t-butyl) peroxide residue.

Provenance & Evidence