HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 20368075, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 20368067 | HCID 20368067 | — |
| Reactant | HCID 178515173 | HCID 178515173 | — |
| Product | HCID 20368075 | HCID 20368075 | 76% |
Reaction Steps
By treating 6-chloropyrazolo[1,5-a]pyrido[4,3-d]pyrimidin-9(4H)-one of Example 1 with methyl iodide according to the procedure of Example 5 for the preparation of 6-chloro-2,4-dimethylpyrazolo[1,5-a]pyrido[4,3-d]pyrimidin-9(4H)-one, 6-chloro-4-methylpyrazolo[1,5-a]pyrido[4,3-d]pyrimidin-9(4H)-one is obtained, yield: 76%; m.p. >300°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04075210 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-86c7912cce7a4b67b8f215a68b9115b0 |
| Source note | uspto-grants-1978_02 |