Phenacyl bromide → 5-Phenacylthieno(3,2-c)pyridinium bromide

HRID 616587Notes

Reaction equation

HRID 616587 reaction equation
[S:1]1[C:9]2[CH:8]=[CH:7][N:6]=[CH:5][C:4]=2[CH:3]=[CH:2]1.[CH2:10]([Br:19])[C:11]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)=[O:12]>CC(C)=O>[Br-:19].[CH2:10]([N+:6]1[CH:7]=[CH:8][C:9]2[S:1][CH:2]=[CH:3][C:4]=2[CH:5]=1)[C:11]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)=[O:12]

Participants

4

Reactant 2

HCID 6259Phenacyl bromideHCID 67500Thieno(3,2-c)pyridine

Product 1

HCID 30413145-Phenacylthieno(3,2-c)pyridinium bromide

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of thieno[3,2-c]pyridine (13.5 g; 0.10 mole) and phenacyl bromide (19.9 g) (0.10 mole) in acetone (200 ml) is stirred for two hours at room temperature.

Sources & evidence

ORD record
ord-59a4870e0c0347c29f80a0cf17303718
Source dataset
uspto-grants-1978_02
Patent number
US04075215

Reaction notes

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