Phenacyl bromide → 2-Chloro-5-(2-oxo-2-phenylethyl)-5H-thieno[3,2-c]pyridin-1-ium bromide

Participants

Role	Name	HCID	Charge
Reactant	Phenacyl bromide	HCID 6259	—
Reactant	2-Chlorothieno[3,2-c]pyridine	HCID 598192	—
Product	2-Chloro-5-(2-oxo-2-phenylethyl)-5H-thieno[3,2-c]pyridin-1-ium bromide	HCID 3041317	80.1%

Reaction Steps

Reaction of 2-chloro-thieno[3,2-c]pyridine (17 g) with phenacyl bromide (20 g) according to the procedure of Example 1 gives white crystals (29.60 g) having a melting point (Koefler block of 239° C.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US04075215
Source dataset	uspto-grants-1978_02
ORD ID	ord-7831469e428742619ff225c0994849b5
Source note	uspto-grants-1978_02