Hydrochloric Acid → HCID 20368556, compound
Reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:9]([CH:15]([NH2:17])[CH3:16])[C:10](OCC)=[O:11])[CH:5]=[CH:6][C:7]=1[Cl:8].Cl>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:9]([CH:15]([NH2:17])[CH3:16])[CH2:10][OH:11])[CH:5]=[CH:6][C:7]=1[Cl:8]Participants
3
Procedure
The compound is prepared according to the procedure described in Example 2, using as starting material 5.5 g. of ethyl 2-(3,4-dichlorophenyl)-3-aminobutyrate. Yield 3.75 g.; boiling point 125° C/0.2 mm Hg. The hydrochloride melts at 157°-160° C.
Workup
- customThe compound is prepared
Sources & evidence
- ORD record
- ord-073d6ad834084dd98318349fb2d922c3
- Source dataset
- uspto-grants-1978_02
- Patent number
- US04075241
Reaction notes
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