HRID616668

反应详情

EQUATION

反应方程式

HRID 616668 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

In the manner given in Example 1, a solution of 8-methylthio-1-methyl-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine in dimethylformamide N,N,N',N',-tetramethyldiaminomethane and acetyl chloride (in 0.1 molar excess compared to the N,N,N',N',-tetramethyldiaminomethane) are reacted together to give 8-methylthio-1-[2-(dimethylamino)ethyl]-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine

WORKUP

后处理

  1. customare reacted together