HRID616952

反应详情

EQUATION

反应方程式

HRID 616952 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

210 g of p-methoxybenzyl bromide and 40 g of potassium iodide are added to 114 g of 2-(hydroxymethyl)pyrazolo[1,5-c]-quinazolin-5(6H)-one and 276 g of potassium carbonate in 2 1. of methanol. After refluxing for 5 hours, the reaction is cooled, poured into 6 1. of water and the title compound is filtered off and dried.

WORKUP

后处理

  1. temperatureAfter refluxing for 5 hours
  2. temperaturethe reaction is cooled
  3. additionpoured into 6 1
  4. filtrationof water and the title compound is filtered off
  5. customdried