N-Phenyldodecanamide → N-Dodecylaniline

HRID 616987Notes

Reaction equation

HRID 616987 reaction equation
[C:1]([NH:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)(=O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].B#B>CCCCCC>[CH2:1]([NH:14][C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

4

Reactant 2

HCID 94794N-Phenyldodecanamide2×HCID 6328200Diboron

Product 1

HCID 76362N-Dodecylaniline

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

N-dodecylaminobenzene was prepared from the N-dodecanoylaminobenzene of (a) by reduction with diborane by a procedure similar to that of Example 1(b). A yield of 74% of white crystals from hexane, m.p. 26.7°-27.2° C. was obtained.

Sources & evidence

ORD record
ord-9a785165bbbf440ea147a2bfbe04a22c
Source dataset
uspto-grants-1978_02
Patent number
US04076849

Reaction notes

Loading…