HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Phenyldodecanamide → N-Dodecylaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Phenyldodecanamide | HCID 94794 | — |
| Reactant | Diboron | HCID 6328200 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | N-Dodecylaniline | HCID 76362 | — |
Reaction Steps
N-dodecylaminobenzene was prepared from the N-dodecanoylaminobenzene of (a) by reduction with diborane by a procedure similar to that of Example 1(b). A yield of 74% of white crystals from hexane, m.p. 26.7°-27.2° C. was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04076849 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-9a785165bbbf440ea147a2bfbe04a22c |
| Source note | uspto-grants-1978_02 |