2-Bromoethanol → HCID 66834128, compound

HRID 61703Notes

Reaction equation

HRID 61703 reaction equation
[OH:1][C:2]1[CH:3]=[CH:4][C:5]2[C:17](=[O:18])[C:16]3[C:15]4[C:10](=[CH:11][C:12]([C:19]#[N:20])=[CH:13][CH:14]=4)[NH:9][C:8]=3[C:7]([CH3:22])([CH3:21])[C:6]=2[CH:23]=1.Br[CH2:25][CH2:26][OH:27]>>[OH:27][CH2:26][CH2:25][O:1][C:2]1[CH:3]=[CH:4][C:5]2[C:17](=[O:18])[C:16]3[C:15]4[C:10](=[CH:11][C:12]([C:19]#[N:20])=[CH:13][CH:14]=4)[NH:9][C:8]=3[C:7]([CH3:21])([CH3:22])[C:6]=2[CH:23]=1

Participants

3

Reactant 2

HCID 108982-BromoethanolHCID 668338618-Hydroxy-6,6-dimethyl-11-oxo-6,11-dihydro-5H-benzo[b]carbazole-3-carbonitrile

Product 1

HCID 66834128HCID 66834128, compound

Procedure

Under the same conditions as the method for synthesizing Compound A7-17, the title compound was prepared from Compound A6 and 2-bromo-ethanol.

Workup

  1. customUnder the same conditions as the method for synthesizing Compound A7-17

Sources & evidence

ORD record
ord-d810174b918b44b8ac9f30d1743b782f
Source dataset
uspto-grants-2016_09
Patent number
US09440922B2

Reaction notes

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