HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 53636566, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Boc-D-valinol | HCID 11241137 | — |
| Product | HCID 53636566 | HCID 53636566 | 67% |
Reaction Steps
The title compound has been prepared in 67% yield from the alcohol of Example 6, Step B and methyl iodide following the alkylation method given in Example 6, Step C. Rf: 0.27 (silica gel, ethyl acetate/petroleum ether: 1/9).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05948778 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-80da9f7ca8174d6193da012395a78f3d |
| Source note | uspto-grants-1999_09 |