HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 21851289, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Reactant | HCID 21851294 | HCID 21851294 | — |
| Product | HCID 21851289 | HCID 21851289 | 83% |
Reaction Steps
The same procedure as in Example 1 was repeated, except that 2.5 g (4.87 mmol) of Compound m obtained in Reference Example 10 was used, and N-methylpyrrolidinone was used as the solvent in place of dimethylformamide, to give 2.29 g (yield: 83%) of Compound n as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05948784 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-016acae43bb6462ca42aa86b9dfc7fc9 |
| Source note | uspto-grants-1999_09 |