HRID617212
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Conc. sulfuric acid was added to a mixture of 2-amino-4,5,3',4'-tetramethoxybenzophenone, butyl acetoacetate and acetic acid. The resulting mixture was treated according to the same manner as that described in Reference Example 1 to obtain butyl 6,7-dimethoxy-4-(3,4-dimethoxy- phenyl)-2-methylquinoline-3-carboxylate (53%) which was recrystallized from ethyl acetate/hexane.
WORKUP
后处理
- additionThe resulting mixture was treated