HRID617212

反应详情

EQUATION

反应方程式

HRID 617212 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Conc. sulfuric acid was added to a mixture of 2-amino-4,5,3',4'-tetramethoxybenzophenone, butyl acetoacetate and acetic acid. The resulting mixture was treated according to the same manner as that described in Reference Example 1 to obtain butyl 6,7-dimethoxy-4-(3,4-dimethoxy- phenyl)-2-methylquinoline-3-carboxylate (53%) which was recrystallized from ethyl acetate/hexane.

WORKUP

后处理

  1. additionThe resulting mixture was treated