HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → Butyl 4-(3,4-dimethoxyphenyl)-6,7-dimethoxy-2-methylquinoline-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Butyl acetoacetate | HCID 11576 | — |
| Reactant | 2-Amino-4,5,3',4'-tetramethoxybenzophenone | HCID 9926967 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Butyl 4-(3,4-dimethoxyphenyl)-6,7-dimethoxy-2-methylquinoline-3-carboxylate | HCID 21851183 | 53% |
Reaction Steps
Conc. sulfuric acid was added to a mixture of 2-amino-4,5,3',4'-tetramethoxybenzophenone, butyl acetoacetate and acetic acid. The resulting mixture was treated according to the same manner as that described in Reference Example 1 to obtain butyl 6,7-dimethoxy-4-(3,4-dimethoxy- phenyl)-2-methylquinoline-3-carboxylate (53%) which was recrystallized from ethyl acetate/hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05948782 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-b28c7f3e854b4831b7b7b7b77478a728 |
| Source note | uspto-grants-1999_09 |