Hydrochloric Acid → HCID 9928264, compound

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Reaction Steps

Using a procedure similar to that described in Example 3, except replacing the 1a used therein with the 1c, the title compound was prepared; 1H NMR (free base) (CDCl3): δ 1.40-2.05 (m, 4H, CH2), 2.45 (m, 2H, CH2), 2.98-3.65 (m, 3H, CH2 and NH), 3.80 (s, 3H, OCH3),4.28 (t, 1H, CH), 6.71-6.81 (m, 3H, Ar--H), 7.0 (d, 1H, Ar--H), 7.21-7.38 (m, 2H, Ar--H). Elemental analysis calcd. for Cl19H19Cl2NO.HCl: C, 59.52; H, 5.26; N, 3.66. Found: C, 59.61; H, 5.57; 2.95.

Provenance & Evidence