Hydrochloric Acid → HCID 67585873, compound

Participants

Reaction Steps

The compound from step 78a above was treated with HCl in ether according to Example 14c to afford 20 mg of the title compound. MS (DCI/NH3) m/e: 211 (M+H)+. 1H NMR (CD3OD, 300 MHz) δ: 8.77 (d, J=2.6 Hz, 1H), 8.57 (d, J=5.5 Hz, 1H), 8.37 (m, 1H), 8.08 (m, 1H, 5.60-5.40 (m, 1H), 4.72 (m, 1H), 4.58 (m, 1H), 4.21 (m, 1H), 4.04 (m, 1H), 3.65-3.47 (m, 1H), 3.19 (s, 3H), 3.02-2.80 (m, 1H), 2.43-2.28 (m, 1H). Anal. Calc. for C11H15N2OF.2.4 HCl.0.2 H2O: C, 43.84; H, 5.95; N, 9.29; Found C, 43.47; H, 5.88; N, 8.98.

Provenance & Evidence