Hydrochloric Acid → HCID 67586036, compound

HRID 617361Notes

Reaction equation

HRID 617361 reaction equation
[N+]([C:4]1[CH:5]=[N:6][CH:7]=[C:8]([N+:10]([O-:12])=[O:11])[CH:9]=1)([O-])=O.[CH3:13][N:14]1[CH2:18][CH2:17][CH2:16][C@H:15]1[CH2:19][OH:20].[ClH:21]>CCOCC>[ClH:21].[ClH:21].[CH3:13][N:14]1[CH2:18][CH2:17][CH2:16][C@H:15]1[CH2:19][O:20][C:4]1[CH:5]=[N:6][CH:7]=[C:8]([N+:10]([O-:12])=[O:11])[CH:9]=1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 5980543,5-DinitropyridineHCID 643492(2S)-1-Methyl-2-pyrrolidinemethanol

Product 1

HCID 67586036HCID 67586036, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

A sample of 3,5-dinitro pyridine from step 93a above is reacted with (S)-(-)-1-methyl-2-pyrrolidinemethanol according to the procedure of Example 3a, and the product is converted into the title compound by treatment with HCl in ether according to Example 14c.

Sources & evidence

ORD record
ord-e05e3069876c42c1a5ca0978ac32ed42
Source dataset
uspto-grants-1999_09
Patent number
US05948793

Reaction notes

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