HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Diethoxyethylamine → HCID 178467937, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Diethoxyethylamine | HCID 69524 | — |
| Reactant | Ethanimidic acid, ethyl ester, hydrochloride (1:1) | HCID 2724290 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178467937 | HCID 178467937 | — |
Reaction Steps
N-(2,2-Diethoxyethyl)acetamidine was synthesized in the same manner as in Reference Example 2. That is, ethyl acetimidate hydrochloride (25.0 g, 0.202 mol) was reacted with aminoacetaldehyde diethyl acetal (31 mL, 0.21 mol) in ethanol (150 mL) to give 44.1 g of a pale-green oil containing the target compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05948785 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-501bf98ba4514f399594e3d758e0b548 |
| Source note | uspto-grants-1999_09 |