HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Ethyl 4-methoxybenzimidate hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 4-Methoxybenzonitrile | HCID 70129 | — |
| Product | Ethyl 4-methoxybenzimidate hydrochloride | HCID 12270046 | — |
Reaction Steps
Ethyl 4-methoxybenzimidate hydrochloride was synthesized in the same manner as in Reference Example 2. That is, anisonitrile (25.6 g, 0.199 mol) was treated with hydrogen chloride in ethanol (250 mL) to give 40.5 g (94%) of the target compound as pale-red crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05948785 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-5314106d1e3e48fdb28b7926bf68f715 |
| Source note | uspto-grants-1999_09 |