HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Pentanol → HCID 21848854, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Pentanol | HCID 22386 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-Acetoxy-2-fluorobenzoic acid | HCID 22721416 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 21848854 | HCID 21848854 | — |
Reaction Steps
Thionyl chloride in an amount of 60 ml was added to 10.8 g (0.06 mol) of 4-acetoxy-2-fluoro-benzoic acid, and the mixture was allowed to react under reflux for 7 hours. Then, excessive thionyl chloride was distilled off, and then 10 ml of pyridine and 3.5 g (0.0402 mol) of 2-pentanol were dropwise added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05951914 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-502012781f764cd1a70576ece2b656e0 |
| Source note | uspto-grants-1999_09 |