HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21849682, compound → HCID 21849672, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21849682 | HCID 21849682 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 21849672 | HCID 21849672 | 31% |
Reaction Steps
This material was prepared from 1,2,3,5,6,7-hexahydro-1-methyl-5'-nitro-7-oxospiro[4H-azepine-4,3'(2H)-benzofuran] (D27, 0.68 g, 2.5 mmol) following the procedure of DESCRIPTION 6, but using acetic acid as solvent. This gave the title compound (0.19 g, 31%) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05952325 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-8a4f9b942352446eb5979cdcbb76fe89 |
| Source note | uspto-grants-1999_09 |