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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 617756Generated: October 30, 2026

HCID 70068774, compound → HCID 18391848, compound

https://huagongshe.com/reaction/617756

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 70068774HCID 70068774—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 18391848HCID 18391848—

Reaction Steps

A solution of (4S)-3,3-diethyl-1-[(R)-α-allyl-(4-methyl)benzylaminocarbonyl]-4-[(4-acetyl)phenoxy]azetidin-2-one (1.3 gm, 2.9 mmol) and 100 mg of 10% palladium on carbon in ethanol (15 mL) was hydrogenated at 40 p.s.i. for 20 min. The reaction was then filtered and evaporated to afford 1.3 gm (quantitative) of clean title compound without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05952321
Source datasetuspto-grants-1999_09
ORD IDord-cf6be66ad26f46d8879ed318bf926b8e
Source noteuspto-grants-1999_09