HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70068774, compound → HCID 18391848, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70068774 | HCID 70068774 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18391848 | HCID 18391848 | — |
Reaction Steps
A solution of (4S)-3,3-diethyl-1-[(R)-α-allyl-(4-methyl)benzylaminocarbonyl]-4-[(4-acetyl)phenoxy]azetidin-2-one (1.3 gm, 2.9 mmol) and 100 mg of 10% palladium on carbon in ethanol (15 mL) was hydrogenated at 40 p.s.i. for 20 min. The reaction was then filtered and evaporated to afford 1.3 gm (quantitative) of clean title compound without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05952321 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-cf6be66ad26f46d8879ed318bf926b8e |
| Source note | uspto-grants-1999_09 |