反应详情

温度

90 °C

4-Decylphenylmethanol (3.91 g) was dissolved in toluene (40 ml) and thereto was added 48% hydrobromic acid (40 ml). The mixture was refluxed under heating at 90° C. for 6 hours. After cooling, the organic layer was separated and washed with saturated brine and a sodium hydrogencarbonate solution. The mixture was dried over anhydrous sodium sulfate and the solvent was distilled away to give 4.9 g of the oily subject compound.

1. temperatureThe mixture was refluxed
2. temperatureAfter cooling
3. customthe organic layer was separated
4. washwashed with saturated brine
5. dry with materialThe mixture was dried over anhydrous sodium sulfate
6. distillationthe solvent was distilled away