HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 12017168, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 12017167 | HCID 12017167 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 12017168 | HCID 12017168 | — |
Reaction Steps
HCl gas was bubbled through a solution of 2-5 (0.8 g, 2.5 mmol) and EtOAc (15 mL) at 0° C. for 15 min. After an additional 15 min argon was passed through the solution for 15 min followed by concentration. The residue was azeotroped twice with ether to give 2-6 as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05952341 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-d920c15dbaa64d3495582398874a3d8f |
| Source note | uspto-grants-1999_09 |