HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Chloromethyl)-5-methyl-1,3-dioxol-2-one → HCID 21850252, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Chloromethyl)-5-methyl-1,3-dioxol-2-one | HCID 9855518 | — |
| Reactant | 170488-48-9 | HCID 9927763 | — |
| Product | HCID 21850252 | HCID 21850252 | 6% |
Reaction Steps
Substantially the same procedure as in Example 3 was repeated using Compound 1 (2.37 g) obtained in Example 1 and 4-chloromethyl-5-methyl-1,3-dioxol-2-one (1.63 g) except that the obtained crude crystals were further purified by preparative high-pressure liquid chromatography (HPLC), to give Compound 11 (188 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05952355 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-fcbca8d85600470fa11cee97121fd54f |
| Source note | uspto-grants-1999_09 |