HuagongsheHuagongshe Chemistry Print Report · For research reference only
3',4',5'-Trimethoxyacetophenone → HCID 21850275, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3',4',5'-Trimethoxyacetophenone | HCID 14345 | — |
| Reactant | 5-Bromoindole-3-carbaldehyde | HCID 70137 | — |
| Product | HCID 21850275 | HCID 21850275 | 65.7% |
Reaction Steps
Substantially the same procedure as in Example 12 was repeated using 3',4',5'-trimethoxyacetophenone (2.1 g) and 5-bromoindole-3-carboxaldehyde (2.24 g) except that the obtained crystals were recrystallized from ethyl acetate, to give Compound 31 (2.73 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05952355 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-b371f75ffa7147a7994d6b4d8df057e5 |
| Source note | uspto-grants-1999_09 |