Hydrochloric Acid → HCID 70248931, compound

Participants

Reaction Steps

HCl gas was passed through a solution of 24-1a (0.84 g, 2.4 mmol) in EtOAc (24 mL) at 0° C. for 15 min and the reaction mixture stirred for an additional 15 min. The reaction mixture was concentrated and the residue triturated with ether to give 24-2 as a white solid.

Provenance & Evidence