HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 21847869, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Reactant | HCID 178418385 | HCID 178418385 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 21847869 | HCID 21847869 | — |
Reaction Steps
A stirred mixture of benzotriazole (3 g), triphosgene (11.22 g), charcoal (1 g) and anhydrous toluene was refluxed overnight and filtered. Evaporation of the filtrate gave an oily solid which was suspended in a mixture of hexane and ether (1:1). Filtration and evaporation of the filtrate gave the titled compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05955470 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-34e0ae09921a4e73b0bf41fef4e4e8fb |
| Source note | uspto-grants-1999_09 |