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HRID618945

反应详情

EQUATION

反应方程式

HRID 618945 的结构方程式

REACTANTS

反应物

1
结构：COc1cc([N+](=O)[O-])cc([N+](=O)[O-])c1
HCID79231

Benzene, 1-methoxy-3,5-dinitro-

C7H6N2O5

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1cc(O)cc([N+](=O)[O-])c1
HCID11459

3,5-Dinitrophenol

C6H4N2O5

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Br
溶剂HCID260

Hydrogen Bromide

BrH

PROCEDURE

实验过程

3,5-Dinitroanisole (1.36 g, 6.9 mmol) and concentrated aqueous HBr (50 ml) was heated to reflux temperature for 16 h. After cooling to ambient temperature, the solid precipitate was filtered off, washed with water and dried. Yield: 325 mg (26%).

WORKUP

后处理

  1. temperatureto reflux temperature for 16 h
  2. filtrationthe solid precipitate was filtered off
  3. washwashed with water
  4. customdried