HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-methoxy-3,5-dinitro- → 3,5-Dinitrophenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-methoxy-3,5-dinitro- | HCID 79231 | — |
| Solvent | Hydrogen Bromide | HCID 260 | — |
| Product | 3,5-Dinitrophenol | HCID 11459 | — |
Reaction Steps
3,5-Dinitroanisole (1.36 g, 6.9 mmol) and concentrated aqueous HBr (50 ml) was heated to reflux temperature for 16 h. After cooling to ambient temperature, the solid precipitate was filtered off, washed with water and dried. Yield: 325 mg (26%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05958375 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-db06cdd2ff2a4ae48ebdfc79d58c2b36 |
| Source note | uspto-grants-1999_09 |