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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 619022Generated: October 31, 2026

Ammonium Hydroxide → HCID 178505164, compound

https://huagongshe.com/reaction/619022

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmonium HydroxideHCID 14923—
ReactantHCID 70099995HCID 70099995—
SolventIsopropanolHCID 3776—
ProductHCID 178505164HCID 178505164—

Reaction Conditions

Temperature25 °C

Reaction Steps

The product of Example 26 is dissolved in 2-propanol and concentrated NH4OH is added. The mixture is stirred at 25° C. for 24 h and then evaporated to dryness. The residue is triturated with Et2O (2×250 ml) and the ether discarded. The resulting product is chromatographed on a silica gel column to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05958890
Source datasetuspto-grants-1999_09
ORD IDord-ad75a8ab77e54b39ad1e33f3a099a171
Source noteuspto-grants-1999_09