HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9837522, compound → HCID 21845565, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9837522 | HCID 9837522 | — |
| Reactant | 2-Bromo-1-(3,4-dihydroxy-5-nitro-phenyl)-ethanone | HCID 21845596 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21845565 | HCID 21845565 | — |
Reaction Steps
A mixture of 0.24 g of N-(aminothioxomethyl)-4-methyl-benzene-sulfonamide and 0.2 g of 2-bromo-1-(3,4-dihydroxy-5-nitrophenyl)ethanone was dissolved in 5 ml of ethanol and boiled under reflux for 1 h. 0.26 g of N-[4-(3,4-dihydroxy-5-nitro-phenyl)-thiazol-2-yl]-4-methyl-benzenesulfonamide separated as red crystals upon cooling.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05958910 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-ddb20a425e244866b1c3680cb05ff0bd |
| Source note | uspto-grants-1999_09 |