HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 67556213, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 2-Dimethylaminopyridine | HCID 21885 | — |
| Reactant | Phenylphosphonic dichloride | HCID 69990 | — |
| Reactant | HCID 53993884 | HCID 53993884 | — |
| Reactant | HCID 86752773 | HCID 86752773 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67556213 | HCID 67556213 | 21% |
Reaction Steps
It is prepared from 4-dodecyloxy-N,N-di(2-hydroxy-3-butoxy)-propyl aniline (5.38 g, 10 mmol), pyridine (3 g, 30 mmol), dimethylaminopyridine (0.2 g) and phenylphosphonic dichloride (2.32 g, 11 mmol) in dichloromethane as described for compound 200 to obtain a white solid 1.44 g (21%) and its isomer 1.4 g (20% a white solid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05958663 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-425259ae1f374251b2e71cf2d1ceeefa |
| Source note | uspto-grants-1999_09 |