HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 86752774, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Phenyl phosphorus dichloride | HCID 12573 | — |
| Reactant | 2-Dimethylaminopyridine | HCID 21885 | — |
| Reactant | HCID 54485562 | HCID 54485562 | — |
| Reactant | HCID 86752773 | HCID 86752773 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86752774 | HCID 86752774 | 24% |
Reaction Steps
It is prepared from 4-methoxy-N,N-di(2-hydroxy-3-butoxy)-propyl aniline (1.91 g, 5 mmol), pyridine (1.2 g, 15 mmol), dimethylaminopyridine (0.2 g) and phenylphosphonous dichloride (1 g, 5.1 mmol) in dichloromethane as described for compound 200 to obtain a colourless liquid 0.6 g (24%) and its isomer 0.6 g (24% a colourless liquid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05958663 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-17f0765332d04b73a19ce0abec337f24 |
| Source note | uspto-grants-1999_09 |